Isopropylhydroxylamine → HCID 85049637, compound

HRID 2303536Notes

Reaction equation

HRID 2303536 reaction equation
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[CH:7]=O)[CH3:2].[CH:14]([NH:17][OH:18])([CH3:16])[CH3:15]>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:17]([CH:14]([CH3:16])[CH3:15])[O-:18])[CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[CH3:2]

Participants

3

Reactant 2

HCID 78763IsopropylhydroxylamineHCID 2447283-Ethoxy-4-methoxybenzaldehyde

Product 1

HCID 85049637HCID 85049637, compound

Procedure

The title compound was prepared according to the procedures described in Examples 11 using 3-ethoxy-4-methoxybenzaldehyde and N-isopropylhydroxylamine. The title compound was isolated in 43.9% yield as a solid, m.p. 80.8° C. (Rf=0.15 on a silica gel plate using ethyl acetate as the eluant).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-f2772e3ac50146f79dc7ceb4ed8cbdb6
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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