4-(Benzyloxy)-3-methoxybenzaldehyde → alpha-(4Benzyloxy-3-methoxyphenyl)-N-n-butylnitrone

HRID 2303541Notes

Reaction equation

HRID 2303541 reaction equation
[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][C:10]=1[O:17][CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:19]([NH:23][OH:24])[CH2:20][CH2:21][CH3:22]>>[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=[N+:23]([CH2:19][CH2:20][CH2:21][CH3:22])[O-:24])=[CH:11][C:10]=1[O:17][CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 755064-(Benzyloxy)-3-methoxybenzaldehydeHCID 10034579N-Hydroxy-1-butanamine

Product 1

HCID 86587897alpha-(4Benzyloxy-3-methoxyphenyl)-N-n-butylnitrone

Procedure

The title compound was prepared according to the procedures described in Examples 11 using 4-benzyloxy-3-methoxybenzaldehyde and N-n-butylhydroxylamine. The title compound was isolated in 41.7% yield as a solid, m.p. 81.2° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-8658a3581179492587a4d2a0bcbf467e
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

Loading…