Benzaldehyde, 2-ethoxy- → alpha-(2-Ethoxyphenyl)-N-n-butylnitrone

HRID 2303542Notes

Reaction equation

HRID 2303542 reaction equation
[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=O)[CH3:2].[CH2:12]([NH:16][OH:17])[CH2:13][CH2:14][CH3:15]>>[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=[N+:16]([CH2:12][CH2:13][CH2:14][CH3:15])[O-:17])[CH3:2]

Participants

3

Reactant 2

HCID 11950Benzaldehyde, 2-ethoxy-HCID 10034579N-Hydroxy-1-butanamine

Product 1

HCID 86587898alpha-(2-Ethoxyphenyl)-N-n-butylnitrone

Procedure

The title compound was prepared according to the procedures described in Examples 11 using 2-ethoxybenzaldehyde and N-n-butylhydroxylamine. The title compound was isolated in 44.5% yield as a liquid.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-b06211fbc1f9456398c9abb48a46dd71
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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