Ethylvanillin → HCID 86587900, compound

HRID 2303544Notes

Reaction equation

HRID 2303544 reaction equation
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[OH:12])[CH:7]=O)[CH3:2].I[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH:20]([NH:23][OH:24])([CH3:22])[CH3:21]>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:23]([CH:20]([CH3:22])[CH3:21])[O-:24])[CH:9]=[CH:10][C:11]=1[O:12][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH3:2]

Participants

4

Reactant 3

HCID 8467EthylvanillinHCID 125271-IodohexaneHCID 78763Isopropylhydroxylamine

Product 1

HCID 86587900HCID 86587900, compound

Procedure

The title compound was prepared according to the procedure described in Example 28 using 3-ethoxy-4-hydroxybenzaldehyde, 1-iodohexane and N-isopropylhydroxylamine. The title compound was isolated in 47.1% overall yield as a solid, m.p. 69.0° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-4848bd72698543819b72b24bc504356f
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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