Cyclohexylhydroxylamine → alpha-(2,4,6-Triethoxyphenyl)-N-cyclohexylnitrone

HRID 2303547Notes

Reaction equation

HRID 2303547 reaction equation
[CH2:1]([O:3][C:4]1[CH:11]=[C:10]([O:12][CH2:13][CH3:14])[CH:9]=[C:8]([O:15][CH2:16][CH3:17])[C:5]=1[CH:6]=O)[CH3:2].[CH:18]1([NH:24][OH:25])[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1>>[CH2:1]([O:3][C:4]1[CH:11]=[C:10]([O:12][CH2:13][CH3:14])[CH:9]=[C:8]([O:15][CH2:16][CH3:17])[C:5]=1[CH:6]=[N+:24]([CH:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1)[O-:25])[CH3:2]

Participants

3

Reactant 2

HCID 72935CyclohexylhydroxylamineHCID 2897412,4,6-Triethoxybenzaldehyde

Product 1

HCID 86587902alpha-(2,4,6-Triethoxyphenyl)-N-cyclohexylnitrone

Procedure

The title compound was prepared according to the procedure described in Example 11 using 2,4,6-triethoxybenzaldehyde and N-cyclohexylhydroxylamine. The title compound was isolated in 87.4% yield as a solid, m.p. 145.7° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-d0d02780322c49a4bff013f18f2a35ca
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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