HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methoxybenzaldehyde → alpha-(2-methoxyphenyl)-N-t-butylnitrone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Edukt | N-tert-butylhydroxylamine | HCID 98586 | — |
| Produkt | alpha-(2-methoxyphenyl)-N-t-butylnitrone | HCID 85447185 | — |
Reaktionsschritte
The title compound was prepared according to the procedure described in Example 7 using 2-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.9% overall yield as white crystals, m.p. 109.1° C. (Rf=0.53 on a silica gel plate using ethyl acetate as the eluant).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06433008B1 |
| Quelldatensatz | uspto-grants-2002_08 |
| ORD ID | ord-5e1cce7b983140e695bd0406630df580 |
| Quellennotiz | uspto-grants-2002_08 |