3-Methoxybenzaldehyde → T-BUTYLNITRONE,A-(3-METHOXYPHENYL)

HRID 2303563Notes

Reaction equation

HRID 2303563 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH:6]=O.[C:11]([NH:15][OH:16])([CH3:14])([CH3:13])[CH3:12]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:6]=[N+:15]([C:11]([CH3:14])([CH3:13])[CH3:12])[O-:16])[CH:8]=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 115693-MethoxybenzaldehydeHCID 98586N-tert-butylhydroxylamine

Product 1

HCID 85447184T-BUTYLNITRONE,A-(3-METHOXYPHENYL)

Procedure

The title compound was prepared according to the procedure described in Example 11 using 3-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 56.5% overall yield as a crystalline solid, m.p. 93.4° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-1c94fb85cace4737ab153fc1c2f0fb79
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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