HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54280196, compound → HCID 54455803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54280196 | HCID 54280196 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54455803 | HCID 54455803 | 37% |
Reaction Steps
A mixture of 3 grams of mangenese dioxide and 3 grams of 5-fluoro-2,3-dihydro-1H-indole-6-sulfonic acid amide in 30 ml of dioxane was heated at 50° overnight. The reaction was filtered and the filtrate was evaporated to afford crude product which was purified on silica gel eluting with methylene chloride/ethyl acetate to give 1.1 grams of the titled compound. mp: 181-182° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06433009B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b30feb8ad56f41a0b12dbfa5ebb6a1e0 |
| Source note | uspto-grants-2002_08 |