HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 86758447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 18461338 | HCID 18461338 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86758447 | HCID 86758447 | — |
Reaction Steps
A mixture of t-butyl N-{2-[4-(2,4-dioxothiazolidin-5-ylmethyl)phenoxyacetylamino]-5-(4-benzyl-3-hydroxyphenoxy)phenyl}-N-methylcarbamate (1.4 g) and 4N hydrogen chloride/dioxane (20 ml) was stirred at ambient temperature for 3 days. On addition of ethyl acetate and n-hexane insoluble product was formed and isolated by filtration to give the title compound (1.5 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-20678788d0b9408598e54cf3740efbea |
| Source note | uspto-grants-2002_08 |