Pyridine → HCID 18461413, compound

HRID 2303845Notes

Reaction equation

HRID 2303845 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([OH:8])[CH:5]=[C:4]([CH3:9])[C:3]=1[OH:10].[C:11](Cl)(=[O:16])[C:12]([CH3:15])([CH3:14])[CH3:13].N1C=CC=CC=1>ClCCl>[CH3:1][C:2]1[CH:7]=[C:6]([O:8][C:11](=[O:16])[C:12]([CH3:15])([CH3:14])[CH3:13])[CH:5]=[C:4]([CH3:9])[C:3]=1[OH:10]

Participants

5

Reactant 3

HCID 1049PyridineHCID 62493Pivaloyl chlorideHCID 695602,6-Dimethylhydroquinone

Product 1

HCID 18461413HCID 18461413, compoundYield 61%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

By using 6.90 g of 2,6-dimethylbenzene-1,4-diol, 6.63 g of pivaloyl chloride, 11.85 g of pyridine and 60 ml of dichloromethane, reaction and purification were carried out in a similar manner to that described in Reference Example 9, whereby 6.77 g of the title compound were obtained.

Sources & evidence

ORD record
ord-af9cb94fcf274aac826fe63c363ffcb8
Source dataset
uspto-grants-2002_08
Patent number
US06432993B1

Reaction notes

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