4-Hydroxybiphenyl → HCID 18461263, compound

Participants

Reaction Steps

In a similar manner to that described in Reference Example 6, a reaction was carried out using 4-phenylphenol (4.0 g), t-butyl N-(5-chloro-2-nitrophenyl)-N-methylcarbamate (6.5 g), sodium hydride (55 wt. %, 1.13 g) and anhydrous N,N-dimethylformamide (35 ml) and the reaction mixture was purified to give the title compound (5.5 g).

Provenance & Evidence