HuagongsheHuagongshe Chemistry Print Report · For research reference only
t-Butyl N-[5-(3-dimethylaminophenoxy)-2-nitrophenyl]-N-methylcarbamate → HCID 18461351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | t-Butyl N-[5-(3-dimethylaminophenoxy)-2-nitrophenyl]-N-methylcarbamate | HCID 18461334 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461351 | HCID 18461351 | 82.6% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(3-dimethylaminophenoxy)-2-nitrophenyl]-N-methylcarbamate (2.14 g), palladium on carbon (10%, 2.14 g) and methanol (40 ml) and the reaction mixture was purified to give the title compound (1.63 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-a1cacd8f33484faca26d027a0261e6ab |
| Source note | uspto-grants-2002_08 |