HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461270, compound → HCID 18461347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461270 | HCID 18461270 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461347 | HCID 18461347 | 91.8% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-hydroxy-2,3-dimethylphenoxy)-2-nitrophenyl]-N-methylcarbamate (1.90 g), palladium on carbon (10%, 0.20 g) and methanol (20 ml) and the reaction mixture was purified to give the title compound (1.61 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-12970351230f4e49adb225feea65743f |
| Source note | uspto-grants-2002_08 |