HCID 178485983, compound → HCID 18461489, compound

Participants

Reaction Steps

A mixture of a solution of N-[5-(4-benzoyl-3-hydroxyphenoxy)-2-nitrophenyl]-N-methylcarbamate (2.1 g) in methanol/tetrahydrofuran=5/3 (80 ml) and palladium on carbon (20%, 0.5 g) was stirred at ambient temperature under a hydrogen atmosphere for 4 hours. The reaction mixture was filtered to remove the catalyst and the filtrate was concentrated to give the title compound (1.8 g).

Provenance & Evidence