4-Methylbenzenethiol → HCID 131723435, compound

Participants

Reaction Steps

In a similar manner to that described in Reference Example 6, a reaction was carried out using 4-methylthiophenol (0.98 g), t-butyl N-(5-chloro-2-nitrophenyl)-N-methylcarbamate (2.00 g), sodium hydride (55 wt. %, 0.31 g) and anhydrous N,N-dimethylformamide (60 ml) and the reaction mixture was purified to give the title compound (2.56 g).

Provenance & Evidence