HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18537685, compound → HCID 18537663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18537685 | HCID 18537685 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran ethyl acetate | HCID 21939870 | — |
| Product | HCID 18537663 | HCID 18537663 | 101.2% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-t-butoxycarbonylaminophenoxy)-2-nitrophenyl]-N-methylcarbamate (27.7 g), palladium on carbon (10%, 1.07 g) and tetrahydrofuran/ethyl acetate=9/8 (170 ml) and the reaction mixture was purified to give the title compound (26.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b0a8107984b14fc3aa0d3b0257391338 |
| Source note | uspto-grants-2002_08 |