HCID 18462021, compound → HCID 18462017, compound

HRID 2303936Notes

Reaction equation

HRID 2303936 reaction equation
BrC1C=C(CCCC[OH:12])C=CC=1.[N:13]1[CH:18]=[CH:17][CH:16]=[C:15]([C:19]([C:21]2[CH:22]=[C:23]([CH2:27][CH2:28][CH2:29][CH2:30][OH:31])[CH:24]=[CH:25][CH:26]=2)=[O:20])[CH:14]=1>>[N:13]1[CH:18]=[CH:17][CH:16]=[C:15]([C:19]([C:21]2[CH:22]=[C:23]([CH2:27][CH2:28][CH2:29][C:30]([OH:12])=[O:31])[CH:24]=[CH:25][CH:26]=2)=[O:20])[CH:14]=1

Participants

3

Reactant 2

HCID 18462021HCID 18462021, compoundHCID 218954894-(3-Bromophenyl)butan-1-ol

Product 1

HCID 18462017HCID 18462017, compound

Procedure

4-(3-bromophenyl)butanol and 3-pyridylaldehyde were reacted to synthesize 4-[3-(3-pyridylcarbonyl)phenyl]butanol, then the resultant product was oxidized by a similar method as in Example 2(3) to synthesize the desired compound.

Sources & evidence

ORD record
ord-bfa95ae594d64b02b5e53722241a3650
Source dataset
uspto-grants-2002_08
Patent number
US06433167B1

Reaction notes

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