Ethanol → Ethyl 3,4-dichlorophenylacetate

HRID 2303968Notes

Reaction equation

HRID 2303968 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH2:9][C:10]([OH:12])=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8].[CH2:13](O)[CH3:14]>>[Cl:1][C:2]1[CH:3]=[C:4]([CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 702EthanolHCID 798743,4-Dichlorophenylacetic acid

Product 1

HCID 2737422Ethyl 3,4-dichlorophenylacetateYield 90%

Procedure

90.05 g of 3,4-dichlorophenylacetic acid was dissolved in 150 ml of ethanol, and the solution was treated according to the procedure of Example 5 to obtain 101.30 g (90.0% yield) of the title substance.

Workup

  1. additionthe solution was treated
  2. customto obtain 101.30 g (90.0% yield) of the title substance

Sources & evidence

ORD record
ord-da399ecae76b44329dc07bd15916e4d1
Source dataset
uspto-grants-2002_08
Patent number
US06433174B1

Reaction notes

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