HCID 69780336, compound → HCID 69780573, compound

HRID 2304246Notes

Reaction equation

HRID 2304246 reaction equation
[ClH:1].Cl.[NH2:3][CH:4]([CH2:8][C:9]1[CH:18]=[C:17]2[C:12]([CH:13]=[CH:14][N:15]=[C:16]2[NH2:19])=[CH:11][CH:10]=1)[C:5]([OH:7])=[O:6].Cl.Cl.[CH3:22]OC(=O)C(N)CC1C=C2C(=CC=1)C(N)=NC=C2>>[ClH:1].[ClH:1].[CH3:22][O:6][C:5](=[O:7])[CH:4]([NH2:3])[CH2:8][C:9]1[CH:18]=[C:17]2[C:12]([CH:13]=[CH:14][N:15]=[C:16]2[NH2:19])=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 69780336HCID 69780336, compoundHCID 69780590HCID 69780590, compound

Product 1

HCID 69780573HCID 69780573, compound

Procedure

Compound 37i was prepared from 37h using the procedure described for 1j. 1H-NMR 200 MHz (CD3OD) δ: 3.38-3.60 (2H, m), 3.80 (3H, s), 4.52 (1H, t, J=7 Hz), 7.25 (1H, dd, J=7 Hz and J=1 Hz), 7.59 (1H, d, J=7 Hz), 7.87-7.99 (2H, m), 8.48 (1H, br.s).

Sources & evidence

ORD record
ord-731d6569dfb24f6bab15716bc6a282e3
Source dataset
uspto-grants-2002_08
Patent number
US06432955B1

Reaction notes

Loading…