HCID 408360, compound → HCID 22665691, compound
Reaction equation
[CH2:1]([N:8]=[CH:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1[OH:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[BH4-].[Na+].C(NCC1C=CC=CC=1O)C1C=CC=CC=1>>[CH2:1]([NH:8][CH2:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1[OH:18])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Participants
4
Procedure
This compound was prepared from 1.0 g of 2-(benzylimino-methyl)-4-methoxy-phenol and 0.18 g of sodium borohydride using the procedure described 64b. Yield: 1.0 g (oil), EI-MS: 243 (M+).
Sources & evidence
- ORD record
- ord-07f6b9b98fd24f88aa546fbd6979ffe1
- Source dataset
- uspto-grants-2002_08
- Patent number
- US06432955B1
Reaction notes
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