Aniline → HCID 135709857, compound

Participants

Reaction Steps

This compound was prepared using 85 mg (0.5 mmol) of 2-(phenylhydrazono)-malononitrile, which was derived from aniline (10 mL, 107 mmol) and malononitrile (161 mmol) as described in Example 8, and 4-hydrazinobenzoic acid (76 mg, 0.5 mmol). After reacting for 4 hrs, the reaction remained as a slurry; however, analysis of the reaction solution by TLC indicated that no starting material remained. The resulting solid was isolated by filtration, washed with ethanol, and dried to yield 22 mg (14%) of the title compound as a brown solid.

Provenance & Evidence