Diethylamine → Diethylamine

Participants

Reaction Steps

The title compound was prepared as described in Example 1 starting with (C) of Example 1 (2.0 g, 6.4 mmol) and using diethylamine in place of dibutylamine to produce 2.8 g (85% yield) diethylamine in place of dibutylamine to produce 2.8 g (85% yield) of the title compound as the HCl salt, mp 225°-226° C. IR(KBr): 1600 cm−1. MS: 351(MH+). 1H NMR (CD3 OD): δ 7.99-6.81 (m, 10H), 4.24 (t, J=5.7 Hz, 2H), 3.09 (m, 6H), 2.44 (m, 2H), 0.87 (m, 6H).

Provenance & Evidence