Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,3-Diiodopropane | HCID 12314 | — |
| Reactant | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| Product | HCID 46209693 | HCID 46209693 | — |
Reaction Steps
To a 50 mL round bottom flask is added 2,3,3-trimethylindolenine (14.4 mmol) and 1,3-diiodopropane (72.7 mmol) and the mixture is stirred at 60° C. under an atmosphere of nitrogen for 16 hours. The resulting solid is recrystallized from ethanol to give 1-[3-iodopropyl]-2,3,3-trimethyl-3H-indolium iodide (40) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06437141B2 |
|---|
| Source dataset | uspto-grants-2002_08 |
|---|
| ORD ID | ord-8ef0f8f3f5e44f29a66e66669c842f17 |
|---|
| Source note | uspto-grants-2002_08 |
|---|
