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HRID230485

反应详情

EQUATION

反应方程式

HRID 230485 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(C)c(S(=O)(=O)Cl)c(C)c1
HCID13046

2-Mesitylenesulfonyl chloride

C9H11ClO2S

结构：CC(C)(C)OC(=O)N1CCN(c2ccc(N)c(NS(=O)(=O)c3ccccc3)c2)CC1
HCID22272479

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C)c(S(=O)(=O)Nc2ccc(N3CCNCC3)cc2NS(=O)(=O)c2ccccc2)c(C)c1
HCID10207921

未命名化合物

PROCEDURE

实验过程

2,4,6-Trimethyl-N-[2-[(phenylsulfonyl)amino]-4-(1-piperazinyl)phenyl]benzenesulfonamide was synthesized from N-{2-amino-5-(4-t-butyloxycarbonyl-piperazinyl)-phenyl}benzenesulfonamide and 2-mesitylenesulfonylchloride (52 mg, 0.239 mmol) according to general method 3 to give 50 mg of a purple solid. MS (posES-FIA) m/z=Found: 515.3; Calcd 515.17; 1H-NMR δ 7.74 (d, 2H); 7.63-7.46 (m, 3H), 6.92 (s, 2H), 6.74-6.55 (m, 3H), 3.27-3.20 (m, 8H), 2.35 (s, 6H), 2.25 (s, 3H).