3-Phenylpropylamine → HCID 178523280, compound

HRID 2304914Notes

Reaction equation

HRID 2304914 reaction equation
[NH:1]1[C:5]2[CH2:6][CH2:7][CH:8]([C:10]([OH:12])=O)[CH2:9][C:4]=2[N:3]=[CH:2]1.[C:13]1([CH2:19][CH2:20][CH2:21][NH2:22])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[C:13]1([CH2:19][CH2:20][CH2:21][NH:22][C:10]([CH:8]2[CH2:7][CH2:6][C:5]3[NH:1][CH:2]=[N:3][C:4]=3[CH2:9]2)=[O:12])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 162593-PhenylpropylamineHCID 178524172HCID 178524172, compound

Product 1

HCID 178523280HCID 178523280, compound

Procedure

The title compound was prepared by a similar procedure as described in Example 4 from 100 mg of 2-formyl-5-methoxyphenoxyethylpolystyrene (0.55 mmol/g) resin, 4,5,6,7-tetrahydro-1H-benzimidazole-5-carboxylic acid (111 mg, 0.55 mmol) and 3-phenylpropylamine (74.4 mg, 0.55 mmol).

Sources & evidence

ORD record
ord-ad2023fdac6e40d1a229d0ebdf809701
Source dataset
uspto-grants-2002_08
Patent number
US06437147B1

Reaction notes

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