HCID 14122791, compound → Cyclohexane, nonyl-

HRID 2305004Notes

Reaction equation

HRID 2305004 reaction equation
[H][H].C1OC1.[CH2:6]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1O)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>C1OC1.C(C1(O)CCCCC1)CCCCCCCC>[CH2:6]([CH:15]1[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]1)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

4

Reactant 2

HCID 14122791HCID 14122791, compound2×HCID 178418361HCID 178418361, compound

Product 1

HCID 17900Cyclohexane, nonyl-

Reagents, catalysts & solvents 1

HCID 18459385HCID 18459385, compoundSolvent

Procedure

The consumed amount of hydrogen during the reaction was 136.6 mmoles and was 3.01 moles per 1 mole of charged nonylphenol ethylene oxide adduct. Nonylphenol ethylene oxide adduct residual in nonylcyclohexanol ethylene oxide adduct was determined by liquid chromatography. The amount was 120 ppm by weight. Further, nonylcyclohexane formed by hydrogenation decomposition reaction was determined by gas chromatography. The amount was 150 ppm by weight.

Sources & evidence

ORD record
ord-421d4f5f34804a5f9c4bdaf9a548a2f0
Source dataset
uspto-grants-2002_08
Patent number
US06437194B2

Reaction notes

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