HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Toluenesulfonyl chloride → HCID 10143499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Toluenesulfonyl chloride | HCID 8623 | — |
| Reactant | N-(2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide | HCID 22272501 | — |
| Product | HCID 10143499 | HCID 10143499 | — |
Reaction Steps
The compound was synthesized from of N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide and o-toluenesulfonylchloride (51 mg, 0.269 mmol) to give 18 mg as purple-solid. M+1 501.3 Calcd 501.15; 1HNMR δ 7.78-7.17 (m, 9H), 6.68-6.35 (m, 3H), 3.63-3.10 (m, 8H), 2.59 (s, 3H), 2.09-2.01 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07566715B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-e5d73e80f7bd4f6890c06ab222495424 |
| Source note | uspto-grants-2009_07 |