HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → sodium 2-(4-(N-salicyloyl)aminophenyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-(4-(N-salicyloyl)aminophenyl)propionic acid | HCID 9817303 | — |
| Solvent | Water | HCID 962 | — |
| Product | sodium 2-(4-(N-salicyloyl)aminophenyl)propionate | HCID 23700501 | 92.1% |
Reaction Steps
A solution of 53.05 g (0.186 mol) of 2-(4-(N-salicyloyl)aminophenyl)propionic acid and 300 ml of ethanol was treated with 7.59 g (0.190 mol) of NaOH dissolved in 22 ml of water. The reaction mixture was stirred for 30 min at 25 C. and for 30 min at 0° C. The resulting pale yellow solid was isolated by filtration to give 52.61 g of sodium 2-(4-(N-salicyloyl)aminophenyl)propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06440929B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-2b039e8a662841019b8ce95b0de1c936 |
| Source note | uspto-grants-2002_08 |