Water → HCID 18432350, compound

Participants

Reaction Steps

0.8 g (2.2 mmol) of 2-(4,4,8-trimethyl-1,1-dioxothiochroman-7-yl)carbonyl-1,3-cyclohexanedione was dissolved in 10 ml of methylene chloride, and 0.17 g (2.2 mmol) of pyridine and 0.31 g (2.2 mmol) of benzoyl chloride was added. The mixture was stirred at room temperature for 2 hours, water was added, and the organic phase was separated off, extracted with 2 N hydrochloric acid and dried. The solvent was subsequently distilled off and the residue was chromatographed over silica gel.

Provenance & Evidence