Methyl iodide → HCID 178456402, compound

HRID 2305309Notes

Reaction equation

HRID 2305309 reaction equation
[CH:1](=[N:8][N:9]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][CH3:16])[C:10]1=NC)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C[I:20].[C:21](#[N:23])C>>[I-:20].[CH:1](=[N:8][N:9]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][CH3:16])[C:10]1=[CH:21][NH3+:23])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 6328Methyl iodideHCID 6342AcetonitrileHCID 542477831-Benzylideneamino-2-methylimino-3-propyl-imidazolidine

Product 1

HCID 178456402HCID 178456402, compound

Procedure

A mixture of 0.51 g of 1-benzylideneamino-2-methylimino-3-propyl-imidazolidine in 15 ml of acetonitrile with 0.36 g of methyliodide is refluxed for ca. one hour and the solvent is evaporated off. The residue is treated with acetonitrile and the solvent is evaporated off. (1-benzylideneamino-3-propyl-imdazolidine-2-yliden)methyl-ammonium iodide is obtained in the form of a powder.

Workup

  1. temperatureis refluxed for ca. one hour
  2. customthe solvent is evaporated off
  3. additionThe residue is treated with acetonitrile
  4. customthe solvent is evaporated off

Sources & evidence

ORD record
ord-22593d6d99b341f3823de4f7a6223122
Source dataset
uspto-grants-2002_08
Patent number
US06440957B1

Reaction notes

Loading…