HRID2305309

反应详情

EQUATION

反应方程式

HRID 2305309 的结构方程式

PROCEDURE

实验过程

A mixture of 0.51 g of 1-benzylideneamino-2-methylimino-3-propyl-imidazolidine in 15 ml of acetonitrile with 0.36 g of methyliodide is refluxed for ca. one hour and the solvent is evaporated off. The residue is treated with acetonitrile and the solvent is evaporated off. (1-benzylideneamino-3-propyl-imdazolidine-2-yliden)methyl-ammonium iodide is obtained in the form of a powder.

WORKUP

后处理

  1. temperatureis refluxed for ca. one hour
  2. customthe solvent is evaporated off
  3. additionThe residue is treated with acetonitrile
  4. customthe solvent is evaporated off