HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoyl chloride → HCID 18432432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Reactant | 5-Amino-2,4,6-tribromo-1,3-benzenedicarboxylic acid | HCID 18432427 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18432432 | HCID 18432432 | — |
Reaction Steps
50 9 of para-nitrobenzoic acid chloride and 75 g of 5-amino-2,4,6-tribromoisophthalic acid in 400 ml of dioxane are maintained for 18 hours at the reflux temperature. After cooling, the precipitate is filtered off, washed with 50 ml of dioxane and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06440956B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-f017ff2450f94299b502f2bb94ca261f |
| Source note | uspto-grants-2002_08 |