HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydropyran → Ethyl tetrahydro-2H-pyran-2-ylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydropyran | HCID 8894 | — |
| Reactant | HCID 178472844 | HCID 178472844 | — |
| Product | Ethyl tetrahydro-2H-pyran-2-ylacetate | HCID 558877 | — |
Reaction Steps
Following the procedure of Preparative Example 14, 2.0 g (17.5 mmol) of ethyl diazo acetate was reacted with tetrahydropyran to give 1.75 g of the product as a colorless oil, bp 95°-106° C. at 20 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06440974B2 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-fca9b260458d45cb9a1c7223ec674f68 |
| Source note | uspto-grants-2002_08 |