Ethanolamine → HCID 18433052, compound

HRID 2305512Notes

Reaction equation

[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([O:12][CH3:13])=[CH:9][CH:10]=2)[N:5]=[C:4]([C:14]2[CH:19]=[CH:18][C:17]([Cl:20])=[C:16]([Cl:21])[CH:15]=2)[CH:3]=1.[CH2:22]([CH2:24][NH2:25])[OH:23]>>[ClH:1].[Cl:21][C:16]1[CH:15]=[C:14]([C:4]2[CH:3]=[C:2]([NH:25][CH2:24][CH2:22][OH:23])[C:11]3[C:6](=[CH:7][C:8]([O:12][CH3:13])=[CH:9][CH:10]=3)[N:5]=2)[CH:19]=[CH:18][C:17]=1[Cl:20]

Participants

Reactant 2

HCID 700Ethanolamine

HCID 18432976HCID 18432976, compound

Product 1

HCID 18433052HCID 18433052, compound

Procedure

The title compound, m.p. 268-27° C., and MS: m/e=363.0 (M+H+), was prepared from 4-chloro-2-(3,4-dichloro-phenyl)-7-methoxy-quinoline and ethanolamine.

Sources & evidence

ORD record: ord-caa106bee39845e4a391187d1108b92c
Source dataset: uspto-grants-2002_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06440995B1

Reaction notes

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