HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 5-(S)-Azidomethyl-3-[4'-ethylthio-3'-fluorophenyl]oxazolidine-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 5-(S)-Azidomethyl-3-[4'-methylthio-3'-fluorophenyl]oxazolidine-2-one | HCID 22966214 | — |
| Reactant | 5-(S)-azidomethyl-3-[4'-triphenylmethylthio-3'-fluorophenyl]-oxazolidine-2-one | HCID 22966221 | — |
| Product | 5-(S)-Azidomethyl-3-[4'-ethylthio-3'-fluorophenyl]oxazolidine-2-one | HCID 22966212 | — |
Reaction Steps
This compound was prepared analogously to the synthesis of 5-(S)-azidomethyl-3-[4′-methylthio-3′-fluorophenyl]oxazolidine-2-one from iodoethane (0.117 ml, 1.47 mmol) and 5-(S)-azidomethyl-3-[4′-triphenylmethylthio-3′-fluorophenyl]oxazolidine-2-one (0.500 g, 0.979 mmol). Yield 0.267 g (92%). MS (m/z): [M+H]+=297.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06441005B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b6531c67322d440887f2cb89bc6ed8cc |
| Source note | uspto-grants-2002_08 |