4-(Benzyloxy)-3-methoxybenzaldehyde → alpha-(4-Benzyloxy-3-methoxyphenyl)-N-isopropylnitrone

HRID 2305788Notes

Reaction equation

HRID 2305788 reaction equation
[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][C:10]=1[O:17][CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:19]([NH:22][OH:23])([CH3:21])[CH3:20]>>[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=[N+:22]([CH:19]([CH3:21])[CH3:20])[O-:23])=[CH:11][C:10]=1[O:17][CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 755064-(Benzyloxy)-3-methoxybenzaldehydeHCID 78763Isopropylhydroxylamine

Product 1

HCID 86587896alpha-(4-Benzyloxy-3-methoxyphenyl)-N-isopropylnitrone

Procedure

The title compound was prepared according to the procedures described in Examples 11 using 4-benzyloxy-3-methoxybenzaldehyde and N-isopropylhydroxylamine. The title compound was isolated in 54.6% yield as a solid, m.p. 95.5° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-af3199cac67a451bb57037148b362675
Source dataset
uspto-grants-2002_08
Patent number
US06441032B1

Reaction notes

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