Ethylvanillin → HCID 85059889, compound

HRID 2305789Notes

Reaction equation

HRID 2305789 reaction equation
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[OH:12])[CH:7]=O)[CH3:2].I[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH:20]1([NH:26][OH:27])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:26]([CH:20]2[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]2)[O-:27])[CH:9]=[CH:10][C:11]=1[O:12][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH3:2]

Participants

4

Reactant 3

HCID 8467EthylvanillinHCID 125271-IodohexaneHCID 72935Cyclohexylhydroxylamine

Product 1

HCID 85059889HCID 85059889, compound

Procedure

The title compound was prepared according to the procedure described in Example 28 using 3-ethoxy-4-hydroxybenzaldehyde, 1-iodohexane and N-cyclohexylhydroxylamine. The title compound was isolated in 41.3% yield as a solid, m.p. 67.3° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-dc10ac11e6914b34b2c436083bfaf38f
Source dataset
uspto-grants-2002_08
Patent number
US06441032B1

Reaction notes

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