HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)-hexanoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | Ethyl 2-bromohexanoate | HCID 79072 | — |
| Product | 2-(4-Methoxy-phenylsulfanyl)-hexanoic acid ethyl ester | HCID 53708125 | 98% |
Reaction Steps
2-(4-Methoxy-phenylsulfanyl)-hexanoic acid ethyl ester was prepared according to the general method as outlined in Example 1. Starting from ethyl 2-bromo,hexanoate (7 g, 32 mmol) and 4-methoxybenzenethiol (4.2 g, 30 mmol), 8.3 g of the product was isolated. Yield 98%; Light yellow oil; MS: 283 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06441023B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-3aefa22e61d947ebbe8da67f1437dd84 |
| Source note | uspto-grants-2002_08 |