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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2305863Generated: October 31, 2026

HCID 11089050, compound → HCID 70148114, compound

https://huagongshe.com/reaction/2305863

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 11089050HCID 11089050—
SolventMethanolHCID 887—
SolventSodium HydroxideHCID 14798—
ProductHCID 70148114HCID 70148114—

Reaction Steps

2-Allyl-2-(4-methoxy-benzenesulfonyl)-pentenoic acid was prepared starting from 2-allyl-2-(4-methoxy-benzenesulfonyl)-pent-4-enoic acid ethyl ester (2.2 g, 6.5 mmol) dissolved in methanol (50 ml) and 10 N NaOH (30 ml). The resulting reaction mixture was worked up as outlined in Example 9. Yield 1.76 g, 87%; yellowish oil; MS: 311 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06441023B1
Source datasetuspto-grants-2002_08
ORD IDord-d8bc2caedccf44b1ae49ef12d9f4be68
Source noteuspto-grants-2002_08