4,4-Dimethylpiperidine → HCID 53909022, compound

HRID 2306160Notes

Reaction equation

HRID 2306160 reaction equation
[CH2:1]([C@H:3]1[O:5][CH2:4]1)Cl.[CH3:6][C:7]1([CH3:13])[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]1>>[CH3:6][C:7]1([CH3:13])[CH2:12][CH2:11][N:10]([CH2:1][C@H:3]2[CH2:4][O:5]2)[CH2:9][CH2:8]1

Participants

3

Reactant 2

HCID 1381004,4-DimethylpiperidineHCID 149428(+)-Epichlorohydrin

Product 1

HCID 53909022HCID 53909022, compound

Procedure

The compound is prepared analogously to J. Amer. Chem. Soc. 80; 1958, 1257 by reacting (S)-epichlorohydrin with 4,4-dimethylpiperidine, while the reaction temperature should not exceed 35° C.: Boiling point: 101-104° C./15 mbar.

Workup

  1. customThe compound is prepared analogously to J
  2. customexceed 35° C.

Sources & evidence

ORD record
ord-6f42f7d17bf345b69de1da886e5f2f6a
Source dataset
uspto-grants-2002_08
Patent number
US06441237B1

Reaction notes

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