HRID23064

反应详情

EQUATION

反应方程式

HRID 23064 的结构方程式

PROCEDURE

实验过程

Following General Procedure BA above and using phenylacetyl chloride (Aldrich) and D,L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

WORKUP

后处理

  1. customThe reaction was monitored by tlc on silica gel and purification
  2. extractionwas by extraction with Et2O