Water → HCID 22608792, compound

HRID 2306518Notes

Reaction equation

HRID 2306518 reaction equation
[I-].[CH:2]1([N+:12]2([CH3:17])[CH2:16][CH2:15][CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[OH2:18]>>[OH-:18].[CH:2]1([N+:12]2([CH3:17])[CH2:16][CH2:15][CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 962WaterHCID 22608791HCID 22608791, compound

Product 1

HCID 22608792HCID 22608792, compound

Procedure

N-cyclodecyl-N-methyl-pyrrolidinium iodide (45 gm; 0.128 mol) was dissolved in 150 ml water in a 500 ml plastic bottle. To the solution, 160 gm of Ion-Exchange Resin-OH (BIO RAD® AHI-X8) was added and the mixture was stirred at room temperature overnight. The mixture was filtered and the solids were rinsed with an additional 85 ml of water. The reaction afforded 0.12 mole of the SDA (N-cyclodecyl-N-methyl-pyrrolidinium hydroxide) as indicated by titration analysis with 0.1N HCl.

Workup

  1. filtrationThe mixture was filtered
  2. washthe solids were rinsed with an additional 85 ml of water

Sources & evidence

ORD record
ord-e1429ac1264b4b8fabe77ae9b748d5ba
Source dataset
uspto-grants-2004_12
Patent number
US06827843B2

Reaction notes

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