N-Methylbutylamine → HCID 24826945, compound
Reaction equation
[F:1][C:2]([F:22])([F:21])[C:3]1[C:11]2[CH2:10][CH2:9][CH2:8][CH2:7][C:6]=2[N:5]([C:12]2[CH:20]=[CH:19][C:15]([C:16](O)=[O:17])=[CH:14][CH:13]=2)[N:4]=1.[CH3:23][NH:24][CH2:25][CH2:26][CH2:27][CH3:28]>>[CH2:25]([N:24]([CH3:23])[C:16](=[O:17])[C:15]1[CH:14]=[CH:13][C:12]([N:5]2[C:6]3[CH2:7][CH2:8][CH2:9][CH2:10][C:11]=3[C:3]([C:2]([F:21])([F:1])[F:22])=[N:4]2)=[CH:20][CH:19]=1)[CH2:26][CH2:27][CH3:28]Participants
3
Procedure
The title compound was prepared from 4-[3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl]benzoic acid and N-methylbutylamine using a similar procedure to that described for Example 2.
Sources & evidence
- ORD record
- ord-ff2e94ad95fc438d97258fe5fc076cfe
- Source dataset
- uspto-grants-2009_07
- Patent number
- US07566735B2
Reaction notes
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