HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorobenzaldehyde → 3,5-Difluorobenzaldehyde 2-(6-chloro-5-cyclobutyl-3-pyridazinyl)hydrazone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorobenzaldehyde | HCID 588160 | — |
| Reactant | 3-chloro-4-cyclobutyl-6-hydrazinylPyridazine | HCID 22609946 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 3,5-Difluorobenzaldehyde 2-(6-chloro-5-cyclobutyl-3-pyridazinyl)hydrazone | HCID 73985902 | — |
Reaction Steps
3-Chloro-4-cyclobutyl-6-hydrazinopyridazine (0.502 g, 2.53 mmol) and 3,5-difluorobenzaldehyde (285 ml, 2.78 mmol) were stirred in 0.2M hydrochloric acid (10 ml) for 2 hours. This product was then collected by filtration and dried (0.81 g, 99%). MS (ES+) 323 [MH]+, 325 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828322B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-d7cf817594a04c958e3724d6065b1e8c |
| Source note | uspto-grants-2004_12 |