HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-5-(tri-n-butylstannyl)imidazole → (1-Benzyl-1H-indazol-5-yl)-(6-(3-methyl-3H-imidazol-4-yl)-quinazolin-4-yl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-5-(tri-n-butylstannyl)imidazole | HCID 10915651 | — |
| Reactant | (1-Benzyl-1H-indazol-5-yl)-(6-iodoquinazolin-4-yl)-amine | HCID 21952131 | — |
| Product | (1-Benzyl-1H-indazol-5-yl)-(6-(3-methyl-3H-imidazol-4-yl)-quinazolin-4-yl)-amine | HCID 22609868 | — |
Reaction Steps
Prepared in an analogous manner to Example 6 according to Procedure B from (1-Benzyl-1H-indazol-5-yl)-(6-iodoquinazolin-4-yl)-amine and 5-(tributylstannyl)-1-methylimidazole; δH [2H6]DMSO 9.98(1H, s), 8.62(1H, s), 8.55(1H, s), 8.20(1H, s), 8.15(1H, s), 7.99(1H, dd), 7.83(2H, m), 7.70(2H, m), 7.28(6H, m), 5.70(2H, s), 3.70(3H, s); m/z (M+1)+ 432.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828320B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-da1b732a84b64657a116adc865cf7cc8 |
| Source note | uspto-grants-2004_12 |