1-(Phenylmethyl)-1H-indazol-5-amine → HCID 22609849, compound

Participants

Reaction Steps

The crude solid 4-Chloro-7-(5-Methyl-[1,3,4]oxadiazol-2-yl)-quinazoline was suspended in dry acetonitrile. 1-Benzyl-1H-indazol-5-ylamine (0.03 g) was added and the mixture heated at reflux for 18 hours under nitrogen (Procedure A). The mixture was cooled and the title compound collected by filtration; δH [2H6]DMSO 11.82(1H, bs), 9.08(1H, s), 8.99(1H, s), 8.47(1H, s), 8.44(1H, d), 8.37(1H, s), 8.17(1H, s), 7.89(1H, d), 7.72(1H, d), 7.35(5H, m), 5.80(2H, s) 2.72 (3H, s); m/z (M+1+) 434.

Provenance & Evidence