HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22609212, compound → HCID 69896923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22609212 | HCID 22609212 | — |
| Reactant | HCID 22609214 | HCID 22609214 | — |
| Product | HCID 69896923 | HCID 69896923 | — |
Reaction Steps
Following the procedure for the preparation of 10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from 10-(2-phenylethyl)-1,2,3,4,5,6-hexahydroazepino[4,5-b]indole the title compound was prepared: 1H NMR (CDCl3) δ 2.02, 2.14, 2.31, 2.79, 2.88, 2.97, 3.15, 3.64, 4.18, 6.52, 6.70, 7.07, 7.16, 7.21, 7.27, 9.5-9.7. HRMS (FAB) calcd for C20H24N2 (MH+) 293.2018, found 293.2013.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828314B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-f79a76d6644540c4851d26f9fd8dc1dd |
| Source note | uspto-grants-2004_12 |