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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307060Generated: November 2, 2026

HCID 22609212, compound → HCID 69896923, compound

https://huagongshe.com/reaction/2307060

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22609212HCID 22609212—
ReactantHCID 22609214HCID 22609214—
ProductHCID 69896923HCID 69896923—

Reaction Steps

Following the procedure for the preparation of 10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from 10-(2-phenylethyl)-1,2,3,4,5,6-hexahydroazepino[4,5-b]indole the title compound was prepared: 1H NMR (CDCl3) δ 2.02, 2.14, 2.31, 2.79, 2.88, 2.97, 3.15, 3.64, 4.18, 6.52, 6.70, 7.07, 7.16, 7.21, 7.27, 9.5-9.7. HRMS (FAB) calcd for C20H24N2 (MH+) 293.2018, found 293.2013.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06828314B2
Source datasetuspto-grants-2004_12
ORD IDord-f79a76d6644540c4851d26f9fd8dc1dd
Source noteuspto-grants-2004_12