HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22396585, compound → HCID 69896244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22396585 | HCID 22396585 | — |
| Reactant | HCID 22609212 | HCID 22609212 | — |
| Product | HCID 69896244 | HCID 69896244 | — |
Reaction Steps
Following the procedure for the preparation of 10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from 10-(3-phenoxypropyl)-1,2,3,4,5,6-hexahydroazepino[4,5-b]indole the title compound was prepared: 1H NMR (CDCl3) δ 2.02-2.14, 2.27, 2.74, 2.90-3.03, 3.45, 3.50, 3.98, 4.14, 4.50, 6.47, 6.63, 6.91, 6.95, 7.03, 7.30. HRMS (FAB) calcd for C21H26N2O (MH+) 323.2123, found 323.2104.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828314B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-9b9c75c1ef2b497fa31534e0f748358d |
| Source note | uspto-grants-2004_12 |