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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307062Generated: November 2, 2026

HCID 22396585, compound → HCID 69896244, compound

https://huagongshe.com/reaction/2307062

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22396585HCID 22396585—
ReactantHCID 22609212HCID 22609212—
ProductHCID 69896244HCID 69896244—

Reaction Steps

Following the procedure for the preparation of 10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from 10-(3-phenoxypropyl)-1,2,3,4,5,6-hexahydroazepino[4,5-b]indole the title compound was prepared: 1H NMR (CDCl3) δ 2.02-2.14, 2.27, 2.74, 2.90-3.03, 3.45, 3.50, 3.98, 4.14, 4.50, 6.47, 6.63, 6.91, 6.95, 7.03, 7.30. HRMS (FAB) calcd for C21H26N2O (MH+) 323.2123, found 323.2104.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06828314B2
Source datasetuspto-grants-2004_12
ORD IDord-9b9c75c1ef2b497fa31534e0f748358d
Source noteuspto-grants-2004_12