HCID 22396965, compound → HCID 69895366, compound

Participants

Reaction Steps

Following the procedure for the preparation of (5aS*,10bS*)-10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from N-(2-chlorophenyl)-1,2,3,4,5,6-hexahydroazepino[4,5-b]indol-10-amine the title compound was prepared: 1H NMR (DMSO-d6) δ 1.68, 1.77, 1.93, 2.58, 2.73, 2.95, 5.62, 6.20, 6.77-6.82, 6.86, 6.94, 7.14, 7.37. HRMS (FAB) calcd for C18H20ClN3 (MH+) 314.1424, found 314.1422.

Provenance & Evidence