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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 230726Generated: October 31, 2026

6-Bromohexanoic acid → HCID 178433620, compound

https://huagongshe.com/reaction/230726

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Bromohexanoic acidHCID 20210—
Reactant2,3,3-Trimethyl-3H-pyrrolo[2,3-b]pyridineHCID 22266836—
SolventEthyl AcetateHCID 8857—
ProductHCID 178433620HCID 178433620—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of 0.54 g of 2,3,3-trimethyl-3H-pyrrolo[2,3-b]pyridine and 1.32 g of 6-bromohexanoic acid is heated at 120° C. for one hour. Ethyl acetate (10 mL) is added, and the reaction mixture is heated at reflux for 15 minutes, then cooled to room temperature. The supernatant liquid is decanted to yield the product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07566790B2
Source datasetuspto-grants-2009_07
ORD IDord-c425df9276184d2d8be65377c0caa6af
Source noteuspto-grants-2009_07