HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl iodide → HCID 9822841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178519422 | HCID 178519422 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9822841 | HCID 9822841 | 28.2% |
Reaction Steps
In the manner of Example 25, employing [4-(1H-pyrazol-3-yl)-phenyl]-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-methanone (0.98 g), 60% sodium hydride in oil (0.30 g), dimethylformamide (25 ml), and 1-iodobutane (0.60 g), the title compound (0.32 g) was obtained as a crystalline solid, m.p. 122-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831079B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-e2a9b19d8fc34356b59562fb038808dc |
| Source note | uspto-grants-2004_12 |